Synthesis and application of a novel nanomagnetic catalyst with Cl[DABCO-NO2]C(NO2)3 tags in the preparation of pyrazolo[3,4-b]pyridines via anomeric based oxidation
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Campo DC | Valor | Idioma |
---|---|---|
dc.contributor | Catálisis Estereoselectiva en Síntesis Orgánica (CESO) | es_ES |
dc.contributor.author | Afsar, Javad | - |
dc.contributor.author | Zolfigol, Mohammad Ali | - |
dc.contributor.author | Khazaei, Ardeshir | - |
dc.contributor.author | Alonso, Diego A. | - |
dc.contributor.author | Khoshnood, Abbas | - |
dc.contributor.author | Bayat, Yadollah | - |
dc.contributor.author | Asgari, Asiye | - |
dc.contributor.other | Universidad de Alicante. Departamento de Química Orgánica | es_ES |
dc.contributor.other | Universidad de Alicante. Instituto Universitario de Síntesis Orgánica | es_ES |
dc.date.accessioned | 2018-11-15T13:48:36Z | - |
dc.date.available | 2018-11-15T13:48:36Z | - |
dc.date.issued | 2018-12 | - |
dc.identifier.citation | Research on Chemical Intermediates. 2018, 44(12): 7595-7618. doi:10.1007/s11164-018-3576-9 | es_ES |
dc.identifier.issn | 0922-6168 (Print) | - |
dc.identifier.issn | 1568-5675 (Online) | - |
dc.identifier.uri | http://hdl.handle.net/10045/83627 | - |
dc.description.abstract | A novel nanomagnetic catalyst with Cl[DABCO-NO2]C(NO2)3 tags was designed, synthesized and fully characterized by several techniques such as Fourier transform infrared spectroscopy, energy-dispersive X-ray spectroscopy, elemental mapping analysis, thermogravimetric analysis, derivative thermal gravimetric, powder X-ray diffraction patterns, field scanning electron microscopy, high resolution transmission electron microscopy, physical adsorption and desorption of N2 isotherms (BET) and vibrating sample magnetometer. The synthesized nanomagnetic particles were used as an efficient and recyclable catalyst for the one-pot three component condensation reaction of 3-methyl-1-phenyl-1H-pyrazol-5-amine or 3-methyl-1H-pyrazol-5-amine, aryl aldehydes and malononitrile for the synthesis of pyrazolo[3,4-b]-pyridine derivatives under neat conditions. | es_ES |
dc.description.sponsorship | We thank Bu-Ali Sina University, Iran National Science Foundation (INSF) (Grant Number: 95831207), National Elites Foundation, University of Alicante (VIGROB-173, UAUSTI16-03), and the Spanish Ministerio de Economía y Competitividad (CTQ2015-66624-P) for financial support to our research groups. | es_ES |
dc.language | eng | es_ES |
dc.publisher | Springer Netherlands | es_ES |
dc.rights | © Springer Nature B.V. 2018 | es_ES |
dc.subject | Pyrazolo[3,4-b]pyridine | es_ES |
dc.subject | Nanomagnetic catalyst | es_ES |
dc.subject | Fe2O3@SiO2(CH2)3-Cl[DABCO-NO2]C(NO2)3 | es_ES |
dc.subject | Solvent-free | es_ES |
dc.subject | Anomeric-based oxidation | es_ES |
dc.subject.other | Química Orgánica | es_ES |
dc.title | Synthesis and application of a novel nanomagnetic catalyst with Cl[DABCO-NO2]C(NO2)3 tags in the preparation of pyrazolo[3,4-b]pyridines via anomeric based oxidation | es_ES |
dc.type | info:eu-repo/semantics/article | es_ES |
dc.peerreviewed | si | es_ES |
dc.identifier.doi | 10.1007/s11164-018-3576-9 | - |
dc.relation.publisherversion | https://doi.org/10.1007/s11164-018-3576-9 | es_ES |
dc.rights.accessRights | info:eu-repo/semantics/openAccess | es_ES |
dc.relation.projectID | info:eu-repo/grantAgreement/MINECO//CTQ2015-66624-P | - |
Aparece en las colecciones: | INV - CESO - Artículos de Revistas |
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2018_Afsar_etal_ResChemIntermed_final.pdf | Versión final (acceso restringido) | 2,98 MB | Adobe PDF | Abrir Solicitar una copia |
2018_Afsar_etal_ResChemIntermed_preprint.pdf | Preprint (acceso abierto) | 2,67 MB | Adobe PDF | Abrir Vista previa |
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